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4-Bromoanisole (CAS#104-92-7) Umfanekiso ofakiweyo
  • 4-Bromoanisole (CAS#104-92-7) 1

4-Bromoanisole (CAS#104-92-7)

Ipropati yeMichiza:

Ifomula yeemolekyuli C7H7BrO
IMisa yeMolar 187.03
Ukuxinana 1.494 g/mL ku-25 °C (lit.)
Indawo yokunyibilika 9-10 °C (lit.)
Indawo yeBoling 223 °C (lit.)
Indawo yokuflasha 202°F
Ukunyibilika kwamanzi engadibaniyo
Uxinzelelo loMphunga 0.147mmHg ku-25°C
Imbonakalo Ulwelo
Umbala Icacile engenambala ukuya kumthubi kancinane
Merck 14,1428
I-BRN 1237590
Imeko yoGcino Gcina ngaphantsi +30°C.
Uzinzo Izinzile. Ukutsha. Ayihambelani ne-oxidizing agents ezinamandla.
Refractive Index n20/D 1.564(lit.)

Iinkcukacha zeMveliso

Iithegi zeMveliso

Umngcipheko kunye noKhuseleko

Iimpawu ezinobungozi Xn – Iyingozi
Inkcazelo yoKhuseleko S23 – Musa ukuphefumla umphunga.
S24/25-Kuphephe ukudibana nolusu namehlo.
WGK eJamani 2
RTECS BZ8501000
FLUKA BRAND F IIKHOWUDI 8
I-TSCA Ewe
Ikhowudi ye-HS 29093038
Ubutyhefu I-LD50 orl-mus: 2200 mg/kg GISAAA 44(12),19,79

 

Ulwazi lweReference

Sebenzisa izinto ezikrwada zeziqholo kunye nedayi; I-Organic synthesis kunye ne-pharmaceutical intermediates.
isetyenziswa njengenyibilikisi, ikwasetyenziswa kwi-organic synthesis
I-intermediate ye-Fuke drug Taishu.
organic synthesis. Isinyibilikisi.
indlela yokuvelisa 1. Ithathwe kwi-reaction ye-p-bromophenol kunye ne-dimethyl sulfate. I-p-bromophenol yanyibilikiswa kwisisombululo se-sodium hydroxide edibeneyo, yapholiswa ukuya ngaphantsi kwe-10 °c, emva koko i-dimethyl sulfate yongezwa ngokucothayo ngokuvuselela. Ubushushu bokusabela bunokunyuswa ukuya kuma-30 ° C., lufudunyezwe kwi-40-50 ° C. Kwaye luxutywe kwi-2H. Uluhlu lweoli luhlukaniswe, luhlanjwe ngamanzi kuze kube lungathathi hlangothi, lomiswe nge-anhydrous calcium chloride, kwaye ludityaniswe ukuze lufumane umkhiqizo ogqityiweyo. Nge-anisole njengento eluhlaza, ukusabela kwe-bromination kunye ne-bromine kwi-glacial acetic acid yenziwa, kwaye ekugqibeleni yafunyanwa ngokuhlamba kunye ne-distillation phantsi koxinzelelo oluncitshisiweyo.
I-p-bromophenol isetyenziswa njengento ekrwada ukusabela nge-dimethyl sulfate kwisisombululo se-alkaline. Ekubeni i-reaction exothermic, i-dimethyl sulfate yongezwa ngokukhawuleza ukuze ubushushu kwibhafu yokusabela yi-50 ° C. Okanye ngaphantsi. Emva kokugqitywa kwempendulo, umxube wokuphendula wavunyelwa ukuba ume kwaye iileyile zahlulwa. I-organic layer ikhutshwe kwaye ikhutshwe nge-ethanol okanye i-diethyl ether. Isigaba esikhutshwayo sachithwa ukuze kubuyiselwe i-extractant.
udidi izinto eziyityhefu
ibakala lobutyhefu ukutyhefa
Ubutyhefu obuqatha ngomlomo-mouse LD50: 2200 mg / kg; Intraperitoneal-mouse LD50: 1186 mg / kg
iimpawu ezinobungozi bokutsha ezinokutsha kwidangatye elivulekileyo; Umsi onetyhefu webromidi ekutshayo
ugcino kunye neempawu zokuhamba I-warehouse ifakwe umoya kwaye yomiswe kwiqondo lokushisa eliphantsi, ukugcinwa okuhlukeneyo kwezongezo zokutya
arhente yokucima ikharbon diokside, ugwebu, isanti, inkungu yamanzi.
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